Utilized
signals: elastically scattered
electrons - direct beam and diffracted beams
Methods |
Information |
BF/DF-TEM |
Detection
of crystalline areas, defects and grain boundaries, phase
analysis, particle size |
HRTEM |
Direct visualisation of structures and defects |
EFTEM |
Zero-loss filtering |
ED |
Determination
of lattice parameter and crystal symmetry, crystal orientation,
phase analysis |
A
main advantageous characteristic of a transmission
electron microscope is the
possibility to obtain information in real space (imaging mode)
and reciprocal space (diffraction mode) almost simultaneously.
An
introduction
into the function principles of a TEM with
animations can be found on Goodhew's
Matter page
and into theory and practice of TEM on the web site of Rodenburg.
The
potential of HRTEM in combination with electron diffraction for
structure determination is demonstrated on example of a new Zr/Nb/W
oxide.
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